5 edition of NMR Spectroscopy of Polymers in Solution and in the Solid State (Acs Symposium Series) found in the catalog.
October 31, 2002
by An American Chemical Society Publication
Written in English
|The Physical Object|
|Number of Pages||468|
NMR Spectroscopy of Polymers in Solution and in the Solid State: Cheng, H. N., English, Alan D.: Books - or: H. N. Cheng, Alan D. English. Solid-state NMR spectroscopy insoluble compounds (synthetic polymers) very large compounds (requires speciﬁc labels) determination of the structure in the solid-state (vs. liquid-state) determination of the dynamics in the solid-state Imaging techniques spin tomography "In vivo" NMR spectroscopy distribution of metabolites in the body.
Nuclear magnetic resonance (NMR) spectroscopy is a premiere technique for the studies of polymers. It is widely used for polymer identification, quality control, and reaction monitoring to structure determination, polymer morphology, compatibility, chain conformation, dynamics, diffusion, and imaging. The molecular packing in a polymer: fullerene bimolecular crystal is determined using X-ray diffraction (XRD), molecular mechanics (MM) and molecular dynamics (MD) simulations, 2D solid-state NMR.
NMR Spectroscopy of Polymers Innovative Strategies for Complex Macromolecules Edited by H.N. Cheng, Tetsuo Asakura, and Alan English. American Chemical Society. ACS Symposium Series. Both synthetic and natural polymers are covered ; Includes articles on solid-state NMR, solution NMR, melt-state NMR, and NMR imaging. NMR spectroscopy can provide detailed and quantitative information on the functional groups, topology, dynamics and three-dimensional structure of molecules in solution and the solid state. Since the area under an NMR peak is usually proportional to the number of spins involved, peak integrals can be used to determine composition quantitatively.
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This book provides a source of information on all major aspects of NMR spectroscopy of synthetic polymers. It represents a deliberate attempt to pull together the numerous strands of the su High resolution solid-state NMR studies of polymer chemical and physical structures.
NMR Spectroscopy of Polymers in Solution and in the Solid State brings together a variety of papers on both solution and solid state NMR in one convenient volume. Practicing NMR spectroscopists, students, and other newcomers to the field will benefit from the book.
Advances in the NMR Spectroscopy of Polymers: An Overview / H. Cheng and Alan D. English ; 2. Solution and Solid-State NMR Characterization of Ethylene Oxide-Propylene Oxide Composites for Ultra-Low Dielectric Constant Applications / Peter A.
Mirau and Shu Yang ; 3. High-Temperature Solid-State NMR of Cross-Linked, Insoluble, and Unswellable. NMR Spectroscopy of Polymers in Solution and in the Solid State | H. Cheng and Alan D. English (Eds.) | download | B–OK. Download books for free. Find books. Book • 2nd Edition • Chapter 6 - High resolution NMR spectroscopy of polymers in solution.
Pages Select Chapter 7 - Applications of high-resolution solution NMR Chapter 9 - Applications of high-resolution solid-state NMR spectroscopy to polymers. Pages Select Chapter 10 - Mass spectrometry of polymers. The nuclear magnetic resonance (NMR) spectroscopy is a very powerful tool in the chemical characterization, both in solution and in solid state.
With the development of NMR spectrometers more potent field, employing radio frequency pulse, provided the development of studies on materials, especially amorphous materials.
Thus, there was a need to develop techniques to obtain spectra in solid Author: Maria Ines Bruno Tavares. Purchase Multidimensional Solid-State NMR and Polymers - 1st Edition.
Print Book & E-Book. ISBN Solid-state nuclear magnetic resonance (NMR) has long emerged as a valuable technique for characterizing the molecular structure, conformation, and dynamics of polymer chains in various polymer systems.
The principles of the solid-state 13C NMR cross-polarization experiment are described along with corresponding relaxation measurements. The ensuing Author: Antonio Martínez-Richa, Regan L. Silvestri. Nowadays, NMR is widely used in all different areas of polymer science, from chemical analysis in solution and in the solid state, including but not limited to composition, tacticity, branching and end group determination, to morphology of semicrystalline polymers, blends, micro.
NMR Spectroscopy of Polymers in Solution and in the Solid State (ACS Symposium Series (No. )) [Cheng, H. N., English, Alan D.] on *FREE* shipping on qualifying offers. NMR Spectroscopy of Polymers in Solution and in the Solid State (ACS Symposium Series (No.
))Cited by: This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new solution and solid-state methods in polymer science.
NMR of Polymers is written by leading authorities for graduate students and professionals in academia and industry. Introduction to Solid State NMR In solution NMR, spectra consist of a series of very sharp transitions, due to averaging of anisotropic NMR interactions by rapid random tumbling.
By contrast, solid-state NMR spectra are very broad, as the full effects of anisotropic or orientation-dependent interactions are observed in the spectrum.
Solution NMR spectroscopists have taken advantage of NUS methods for some time. – Recently, our group and several others have explored the usefulness of NUS protocols for more efficient collection of solid-state NMR data.
10,12,17 As was originally demonstrated by Rovnyak et al., in an equivalent experiment time, time-domain sensitivity enhancements of twofold are.
The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR. The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter.
In the second part, applications of NMR to a variety of polymer systems in the solid state are es of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book.
This book provides a source of information on all major aspects of NMR spectroscopy of synthetic polymers. It represents a deliberate attempt to pull together the numerous strands of the subject in a single comprehensive volume, designed to be readable at every scientific level.
It is. |t Advances in the NMR Spectroscopy of Polymers: An Overview / |r H. Cheng and Alan D. English -- |g 2. |t Solution and Solid-State NMR Characterization of Ethylene Oxide-Propylene Oxide Composites for Ultra-Low Dielectric Constant Applications / |r Peter A. Mirau and Shu Yang. ISBN: OCLC Number: Description: xiii, pages: illustrations ; 24 cm.
Contents: 1. Advances in the NMR Spectroscopy of Polymers: An Overview / H.N. Cheng and Alan D. English Solution and Solid-State NMR Characterization of Ethylene Oxide-Propylene Oxide Composites for Ultra-Low Dielectric Constant Applications.
NMR Spectroscopy of Polymers in Solution and in the Solid State provides reviews and original papers on the use of nuclear magnetic resonance (NMR) spectroscopy for polymers. Both synthetic and natural polymers are covered. This book also discusses both solution and solid state : $ The chapters in this collection are from papers which were presented at a symposium on solid-state NMR of polymers.
A two-part program on available NMR techniques applicable to solid polymer analysis was presented at the 3rd Chemical Congress of North American held in Toronto, Ontario, June.
another olefin (i.e. butene or octene) Affects mostly solid state properties. • Long chain branching where the length of the branches is on the same scale as that of the backbone. Affects melt state properties (and solid state properties if high enough degree) • Can use 13C-NMR to detect and quantify these different types of branching.Characterization of Polymer Blends with Solid‐State NMR Spectroscopy Mohammad Mahdi Abolhasani University of Kashan, Chemical Engineering Department, Kashan, Iran.2.
NMR lines are extraordinarily sharp, and extraordinarily close together (in energetic terms) compared to higher energy spectroscopic methods. So much so that Heisenberg uncertainty broadening (which is a function of lifetime of a given energy state, and hence relaxation rates) is a dominant feature of many NMR spectra, and can limit our ability.